Search results for "Formation reaction"

showing 2 items of 2 documents

Natural eutectogels: sustainable catalytic systems for C–C bond formation reactions

2021

Natural eutecto gels were prepared combining properties of amino acids with the ones of deep eutectic solvents. Soft materials obtained were fully characterised determining the gel-sol transition temperatures and analysing mechanical and morphological features through rheological measurements and polarised optical microscopy. All eutecto gels were tested as catalytic reaction media for the enantioselective aldol reaction and, the best performing one was also used to carry out the Michael addition. In both cases, eutecto gels proved to have a great potential as sustainable reaction media, allowing to perform processes under mild conditions, obtaining excellent yields and, in some cases, also…

Natural eutecto gelsMaterials scienceEnantioselective synthesisC-C bond formation reactionsSettore CHIM/06 - Chimica OrganicaSustainable catalytic systemssupramolecular gels ionic liquids organocatalysiPollutionCatalysisSolventQuímica OrgánicaAldol reactionRheologyMichael reactionEnvironmental ChemistryOrganic chemistryaldol reactionEnantiomeric excessEutectic system
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Enhancement of Hydrolysis through the Formation of Mixed Heterometal Species: Al3+/CH3Sn3+ Mixtures

2013

ABSTRACT: The hydrolysis of mixed-metal cations (Al3+/CH3Sn3+) was studied in aqueous solutions of NaNO3, at I = 1.00 ± 0.05 mol·dm−3 and T = 298.15 K, by potentiometric technique. Several hydrolytic mixed species are formed in this mixed system, namely, Alp(CH3Sn)q(OH)r with (p, q, r) = (1, 1, 4), (1, 1, 5), (1, 1, 6), (2, 1, 4), (1, 2, 5), (1, 4, 11), (1, 3, 8), and (7, 6, 32). The stability of these species, expressed by the equilibrium: pAl3+ + qCH3Sn3+ + rOH− = Alp(CH3Sn)q(OH)r 3(p+q)−r, βpqr OH, can be modeled by the empirical relationship: log βpqr OH = −3.34 + 2.67p + 9.23(q + r). By using the equilibrium constant Xpqr relative to the formation reaction: pAl(p+q)(OH)r + q(CH3Sn)(p+q…

equilibrium analysiequilibrium analysis; mixed hydrolysis of metal ions; aluminium(III); monomethyltin(IV)monomethyltin(IV)Aqueous solutionChemistryStereochemistryGeneral Chemical EngineeringPotentiometric titrationEmpirical relationships Formation reaction Mixed species Mixed systems Potentiometric techniqueGeneral ChemistryPotentiometric techniqueMedicinal chemistryTurn (biochemistry)HydrolysisMixed systemsMixed speciesMixed systemsMixed speciesEmpirical relationshipsSettore CHIM/01 - Chimica AnaliticaSolubilityaluminium(III)mixed hydrolysis of metal ionFormation reactionEquilibrium constantJournal of Chemical & Engineering Data
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